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Solvent Locations
HowTo Refill the N
2
Dewar
NMR information
Common Impurities in CD
2
Cl
2
Common Impurities in C
6
D
5
Cl
Common Impurities in
THF
-d
8
Temperature Calibration Plots
Drying of Deuterated Solvents
Cost of NMR Solvent per Sample
NMR HowTos
Pulse Calibration
T1 Measurement
NOESY
DQF-COSEY
HMQC /
13
C Coupled HMQC
Homodecoupled
1
H NMR
Computer HowTos
Making ORTEPs with XShell
CHIME Models in Power Point
Making POV-RAY Models
Info For Group Members
NMR of Common Solvent Impurities in THF-
d
8
1
H NMR
13
C NMR
H
2
0
2.90 (s)
CH
2
Cl
2
5.50 (s)
Et
2
O
1.12 (t) 3.39 (q)
C
6
H
5
CH
3
2.31 (s , CH
3
), 7.19 (t, ph),
7.12 (d, ph) 7.09 (t, ph)
C
6
H
6
7.30 (s)
For further information on common impurities in common solvents see,
JOC
1997,
62
7512-7515
